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Semaglutide

GLP-1 Receptor Agonist

Also known as: Ozempic · Wegovy · Rybelsus

A once-weekly GLP-1 analog with FDA approval for type 2 diabetes & obesity. The most widely verified peptide in the Certipep ledger.

Typical Dose

0.5–2.4 mg once weekly (subcutaneous); 7–14 mg daily (oral)

Route

Subcutaneous injection (once weekly); oral tablet

Cycle

Continuous; dose escalation over 16–20 weeks to maintenance

Half-life

~7 days

Storage

Reconstituted: 2–8°C, use within 28 days. Pen devices: 2–8°C (unused), room temp up to 56 days (in-use).

Overview

Semaglutide is a synthetic analog of glucagon-like peptide-1 (GLP-1) with 94% sequence homology to the native hormone. Fatty acid modification & minor substitutions extend its half-life from ~2 minutes (native GLP-1) to approximately 7 days, enabling once-weekly subcutaneous administration or daily oral use.

It acts on GLP-1 receptors in the pancreas (glucose-dependent insulin secretion, glucagon suppression), hypothalamus (appetite reduction, delayed gastric emptying), & cardiovascular system (demonstrated MACE reduction in SUSTAIN-6 & SELECT trials). The result is significant weight loss (15–17% of body weight in STEP trials) & improved glycemic control.

Compounded semaglutide is widely circulated as a research peptide. Certipep testing has confirmed identity via ESI-TOF-MS across multiple manufacturers, with purity variance being the primary quality differentiator.

Quick Start Guide

1

Reconstitute compounded lyophilized semaglutide with the included diluent or bacteriostatic water.

2

Start at 0.25 mg subcutaneously once weekly for 4 weeks (dose escalation reduces GI side effects).

3

Escalate by 0.25–0.5 mg every 4 weeks to a target of 1–2.4 mg/week based on tolerance.

4

Inject into abdomen, thigh, or upper arm. Rotate sites weekly.

5

Refrigerate after reconstitution. Allow to reach room temperature before injecting.

Research Indications

Weight loss / obesity

Most Effective

STEP trials: 15–17% mean body weight reduction vs 2.4% placebo at 68 weeks. STEP 1 showed ~15% loss at 2.4 mg/week.

Type 2 diabetes (glycemic control)

Most Effective

FDA approved; reduces HbA1c by 1.5–2%. SUSTAIN trial program across 7 trials.

Cardiovascular risk reduction

Effective

SELECT trial (2023): 20% reduction in MACE in overweight/obese adults without diabetes.

Non-alcoholic fatty liver disease (NASH)

Moderate

NASH resolution in 59% vs 17% placebo in Phase II. Phase III trials ongoing.

Research Protocols

Weight loss (standard escalation)

16–20 week escalation; then maintain at highest tolerated dose

Dose

0.25 mg → 0.5 mg → 1 mg → 1.7 mg → 2.4 mg

Frequency

Once weekly SubQ

Route

SubQ abdomen/thigh

Increase dose every 4 weeks. Stop escalation if tolerability is poor; stay at current dose for another 4 weeks before trying again.

Glycemic control (T2D)

Continuous

Dose

0.5–1 mg once weekly

Frequency

Once weekly SubQ

Route

SubQ abdomen/thigh

Peptide Interactions

Do not combine; both are injectable GLP-1 agonists. Switching from one to the other requires a washout given the 7-day half-life.

Same class; do not combine.

Side Effects & Safety

Common

  • Nausea (most common, especially during escalation; typically subsides within 4–8 weeks)
  • Vomiting
  • Diarrhea or constipation
  • Decreased appetite
  • Injection site redness or bruising

Uncommon

  • Pancreatitis (rare; discontinue if suspected)
  • Gallbladder disease / cholelithiasis
  • Tachycardia (small increase in resting heart rate)
  • Hypoglycemia (rare without concomitant insulin/sulfonylurea)

When to Stop

  • Personal or family history of medullary thyroid carcinoma or MEN2 (black box warning)
  • Signs of pancreatitis: severe persistent abdominal pain radiating to back
  • Diabetic retinopathy complications
  • Signs of allergic reaction

How to Reconstitute

1

Wipe the vial stopper with an alcohol swab & allow to dry.

2

Draw the prescribed volume of bacteriostatic water or supplied diluent into a syringe.

3

Inject slowly down the inner wall of the vial. Gently swirl; do not shake.

4

Allow to sit for 2–3 minutes if powder does not dissolve immediately; semaglutide can take slightly longer than smaller peptides.

5

Solution should be clear & colorless. Label & refrigerate.

Dosing math: Concentration varies by compounding pharmacy. Common: 5 mg/mL (0.25 mg = 0.05 mL) or 2.5 mg/mL (0.25 mg = 0.1 mL). Confirm concentration on your vial label before drawing.

Quality Indicators

Good — use as normal

  • Crystal clear, colorless solution
  • No particulate after reconstitution

Acceptable

  • Very faint yellowish tint consistent across the batch

Discard immediately

  • Persistent cloudiness
  • Visible particulate
  • Brown or strong yellow discoloration
  • Any doubt about storage integrity

What to Expect

Weeks 1–4 (0.25 mg)

Most users experience nausea in week 1–2. Appetite suppression begins. Weight loss of 0.5–1 kg is typical at this low dose.

Weeks 5–8 (0.5 mg)

GI side effects usually improving. Appetite suppression is more pronounced. 2–4 kg total loss expected.

Weeks 9–16 (1–1.7 mg)

The majority of weight loss occurs in this range. Energy & satiety improvements are stable. Many users notice significant improvement in food noise (intrusive food thoughts).

Weeks 17+ (maintenance)

At 2.4 mg, studies show continued slow loss through 68 weeks. Weight plateaus at a new set point & regain occurs if discontinued.

Community Insights

Self-reported. Reflects user experience, not clinical outcomes.

Research References

Once-Weekly Semaglutide in Adults with Overweight or Obesity (STEP 1)

New England Journal of Medicine · 2021

Phase III RCT; 2.4 mg semaglutide produced 14.9% mean weight loss vs 2.4% placebo at 68 weeks.

doi:10.1056/NEJMoa2032183
Semaglutide & Cardiovascular Outcomes in Obesity without Diabetes (SELECT)

New England Journal of Medicine · 2023

20% reduction in MACE in 17,604 overweight/obese adults without diabetes over 3.3 years.

doi:10.1056/NEJMoa2307563

Verify what you have

Information on this page applies to pharmaceutical-grade peptides. Purity & identity of research-grade products vary. Certipep provides independent ESI-TOF-MS & HPLC analysis with a signed analytical report.

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